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Chem Impex International fmoc dap fmoc oh
Synthesis of the iminoether 2 derived from <t>Fmoc-L-Ala-NH</t> 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; <t>(iii)</t> <t>DIEA/DCM,</t> rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.
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Chem Impex International fmoc asp opp oh
Synthesis of the iminoether 2 derived from <t>Fmoc-L-Ala-NH</t> 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; <t>(iii)</t> <t>DIEA/DCM,</t> rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.
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BOC Sciences fmoc l lys mtt oh
Synthesis of the iminoether 2 derived from <t>Fmoc-L-Ala-NH</t> 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; <t>(iii)</t> <t>DIEA/DCM,</t> rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.
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Alloc Modulo LTD fmoc-dap(n 3 )-oh
Synthesis of the iminoether 2 derived from <t>Fmoc-L-Ala-NH</t> 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; <t>(iii)</t> <t>DIEA/DCM,</t> rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.
Fmoc Dap(N 3 ) Oh, supplied by Alloc Modulo LTD, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Alloc Modulo LTD fmoc-dap(alloc)-oh
Synthesis of the iminoether 2 derived from <t>Fmoc-L-Ala-NH</t> 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; <t>(iii)</t> <t>DIEA/DCM,</t> rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.
Fmoc Dap(Alloc) Oh, supplied by Alloc Modulo LTD, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Bachem fmoc-dap(boc)-oh
Synthesis of the iminoether 2 derived from <t>Fmoc-L-Ala-NH</t> 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; <t>(iii)</t> <t>DIEA/DCM,</t> rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.
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Image Search Results


Synthesis of the iminoether 2 derived from Fmoc-L-Ala-NH 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; (iii) DIEA/DCM, rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.

Journal: Molecules

Article Title: Solid-Phase Synthesis of an Insect Pyrokinin Analog Incorporating an Imidazoline Ring as Isosteric Replacement of a trans Peptide Bond

doi: 10.3390/molecules26113271

Figure Lengend Snippet: Synthesis of the iminoether 2 derived from Fmoc-L-Ala-NH 2 1 , followed by ring formation on solid support: (i) 1.1 eq. triethyloxonium tetrafluoroborate or triethyloxonium hexafluorophosphate in DCM, rt, 2 h; (ii) washing with 1 M KHCO 3 aq., overnight drying over anhydrous MgSO 4 ; (iii) DIEA/DCM, rt, overnight; (iv) Boc 2 O/DIEA, rt, 3 h.

Article Snippet: Fmoc-Ala-OSu, Fmoc-OSu, H-Ala-NH 2 , Rink resin, HBTU, HOBt, DIEA, and Fmoc-Dap(Fmoc)-OH were purchased from ChemImpex, Inc. (Wood Dale, IL, USA) or IRIS Biotech (Marktredwitz, Germany).

Techniques: Derivative Assay